======Halloween Clock Reaction====== **Materials: **{{$demo.materials_description}}\\ **Difficulty: **{{$demo.difficulty_description}}\\ **Safety: **{{$demo.safety_description}}\\ \\ **Categories:** {{$demo.categories}} \\ **Alternative titles:** Old Nassau Reaction ====Summary==== {{$demo.summary}} ====Procedure==== * See method in links below. ====Links==== Halloween clock reaction - Hegelrast: {{youtube>Tv6_IsdnaGg?}}\\ Halloween Clock Reaction - ChemEx LK: {{youtube>E1OX5Psow5M?}}\\ 📄 Halloween Reaction or Old Nassau Reaction - Anne Marie Helmenstine, Ph.D.: [[https://www.thoughtco.com/halloween-or-old-nassau-reaction-604253]]\\ ====Variations==== * Dilute the solutions to slow the reaction and make the timing of color changes longer. ====Safety Precautions==== * Mercury(II) chloride is highly toxic and must be handled with extreme care; wear gloves, goggles, and a lab coat, and conduct the experiment in a fume hood. * Dispose of mercury-containing waste according to institutional hazardous waste guidelines—do not pour down the sink. * Sodium metabisulfite is an irritant; avoid inhaling dust or vapors. * Potassium iodate is an oxidizer; store away from reducing agents and flammable materials. * Use small-scale quantities only and keep students at a safe viewing distance. ====Questions to Consider==== * Why is this reaction classified as a “clock reaction”? (Because there is a timed delay before the dramatic color change occurs.) * What chemical species is responsible for the orange color? (Mercury(II) iodide, HgI₂, precipitate.) * What causes the final blue-black color? (Iodine forming a complex with starch.) * How does changing the concentration of reagents affect the timing of the reaction? (More dilute solutions slow it down; more concentrated solutions speed it up.)