======Making Soap====== **Materials: **{{$demo.materials_description}}\\ **Difficulty: **{{$demo.difficulty_description}}\\ **Safety: **{{$demo.safety_description}}\\ \\ **Categories:** {{$demo.categories}} \\ **Alternative titles:** Saponification and Soap Purification ====Summary==== {{$demo.summary}} ====Procedure==== - Mix coconut oil and sodium hydroxide solution in a beaker. - Heat gently while stirring until water evaporates and soap forms. - Allow the mixture to cool and test the pH of the crude soap. - Add distilled water and then mix in a hot sodium chloride solution. - Decant the liquid using cheesecloth, leaving behind the solid soap. - Test and record the pH of the soap. - Repeat the salt wash two more times, measuring pH after each wash. - Add a few drops of fragrance oil and press the soap between filter paper. - Place the soap in a mold and allow it to dry overnight. ====Links==== Science Experiment | How to make soap | Saponification | Preparation of Soap in Lab | Sodium Soap - Jagdish Kothawade: {{youtube>iFiEmCK36g4?}}\\ Soap Making Tutorial and Recipe for Absolute Beginners (you can do it!) - Elly's Everyday Soap Making: {{youtube>lBc-dWQmFIM?}}\\ 📄 The Chemistry of Clean: Make Your Own Soap to Study Soap Synthesis - Science Buddies: [[https://www.sciencebuddies.org/science-fair-projects/project-ideas/Chem_p096/chemistry/how-to-make-soap]]\\ 📄 DIY: Make Your Own Soap - The Open University: [[https://www.open.edu/openlearn/science-maths-technology/science/chemistry/diy-make-your-own-soap]]\\ ====Variations==== * Measure the pH of the liquid removed during decanting. * Change the boiling time and compare soap yields. * Vary the reaction temperature and measure soap yield. ====Safety Precautions==== * Safety glasses required. * Gloves and lab coat or apron required. * Sodium hydroxide is caustic and can burn skin and eyes. * Never wear contact lenses when handling sodium hydroxide. * If sodium hydroxide contacts skin, wash with water immediately. * If sodium hydroxide gets in the eyes, rinse with water for at least 15 minutes and seek medical help. * Remove and wash clothing splashed with sodium hydroxide. * Use heat sources carefully and avoid splattering. ====Questions to Consider==== * What other oils can be used for soap making? (Examples include olive oil, palm oil, and soybean oil.) * Why is potassium hydroxide sometimes used instead of sodium hydroxide? (It produces softer, liquid soaps.) * What is a micelle? (A spherical structure formed by soap molecules in water that helps trap and remove grease and dirt.) * What is the most common fatty acid in coconut oil? (Lauric acid.) * How does the structure of a soap molecule make it a good cleaner? (It has a hydrophilic end that interacts with water and a hydrophobic end that binds oils and grease.) * What is a triglyceride? (A fat molecule made of glycerol and three fatty acids.)